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The Column
July 19, 2018
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TOP STORY

Injecting Water onto a GC Column: Solving the Mystery of Poor Chromatography

The direct aqueous injection of ethylene glycol is challenging because it can be difficult to attain reproducibility and good peak shape. The large expansion volume of water can cause backflash, carryover can cause inconsistent results, and excess water can extinguish the flame ionization detection (FID) flame. This article describes a robust approach to analyze glycols in aqueous samples, which reduces downtime and maintains sensitivity. read more

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Features

Do You Work in an Amazing Laboratory?

I recently visited a laboratory where the working culture was different to many (perhaps any) that I've ever encountered. It made me reflect on the laboratories that I've worked in, and what makes a good working environment for the rather serious matter of high-quality analytical measurement. read more


Novel Methods Using Mass Spectrometry for Food Safety–From Contamination to Nutrition

This article highlights three events that require new method development to meet various detection needs, ranging from the detection of pesticides such as fipronil and glyphosate, to the detection and quantification of fat-soluble vitamins. read more

News

Determination of Organometal Contaminants Using PTV GC–ICP-MS

Researchers from the Université de Pau et des Pays de l'Adour, in France, have developed a large volume injection method using a programmed temperature vaporization (PTV) injector for the simultaneous determination of mercury, tin, and lead at ultra-trace levels in natural waters using GC–ICP-MS. read more

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Application Notes

SFC Method Development for Chiral Separation of D- and L Amphetamine

This application note shows the development of an SFC method for the chiral separation of D- and L-amphetamine and the analysis of an authentic whole blood sample.
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3-MCPD and Glycidol in Edible Oils

Automated GC/MS determination of 3-MCPD and glycidol in edible oils. Evaporation step helps reach required LODs with standard MSD and removes excess derivatization reagent for improved stability.
/ Learn more /

GC, GCxGC, and TOF-MS for Characterization and Roast Level Differentiation of Coffee

In this study, the Pegasus® BT 4D is used as a powerful tool for nontarget GC or GCxGC-TOF-MS analyses to gain insight and learn about variations in coffee samples.
/ Learn more /

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